Regarding the crude extract, with an average chain length of 15.52 carbons.Mioso et al.Figure 3 – 1H-NMR spectrum of saturated ethylic biodiesel obtained from Schizochytrium sp.AcknowledgmentsThe authors would like to thank the CAPES agency, Bras ia/ Brazil for the PhD doctoral fellowship and towards the European Commission for any Marie Curie Training Website Fellowship, both granted to R.M. Grateful acknowledgement is produced for economic help towards the project SI-697 (ULPAPD-08/01-5) granted by the Canarian government (Agencia Canaria de Investigaci , Innovaci y Sociedad de la Informaci , ACIISI).
organic compoundsActa Crystallographica Section EStructure Reports OnlineISSN 1600-= 92.113 (6) V = 1066.7 (2) A3 Z=4 Mo K radiation= 0.10 mm T = 293 K 0.50 0.36 0.16 mmData collection2-(5-Methyl-1,three,4-oxadiazol-2-yl)phenyl acetate^ Alexsandro F. dos Santos,a MC4R drug Rodrigo Cristiano,a Petronio F. a b Athayde-Filho and Adailton J. Bortoluzzi Depto. de Quimica – Campus I – Universidade Federal da Paraiba, 58051-900 – Joao Pessoa, PB, Brazil, and bDepto. de Quimica – Universidade Federal de Santa Catarina, 88040-900 – Florianopolis, Santa Catarina, Brazil Correspondence e-mail: [email protected] Received 21 January 2014; accepted 9 AprilaEnraf onius CAD-4 diffractometer 1998 measured reflections 1885 independent reflections 1403 reflections with I two(I)Rint = 0.018 three standard reflections every 200 reflections intensity decay: 1RefinementR[F 2 2(F 2)] = 0.044 wR(F two) = 0.136 S = 1.11 1885 reflections 146 parameters H-atom parameters constrained ax = 0.24 e A in = .20 e AKey indicators: single-crystal X-ray study; T = 293 K; imply (C ) = 0.003 A; R factor = 0.044; wR aspect = 0.136; data-to-parameter ratio = 12.9.Information collection: CAD-4 Application (Enraf onius, 1989); cell refinement: SET4 in CAD-4 Software program; data reduction: HELENA (Spek, 1996); program(s) made use of to solve structure: SIR97 (Altomare et al., 1999); system(s) utilised to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: PLATON (Spek, 2009); computer software utilized to prepare material for publication: SHELXL97.Inside the title compound, C11H10N2O3, that is a potential bioactive compound, the benzene and oxadiazole rings are approximately coplanar, with an inter-ring dihedral angle of 4.14 (2) , while the ester plane is rotated out of the benzene plane [dihedral angle = 82.69 (9) ]. Inside the crystal, the molecules kind layers down the a axis with weak interactions among the oxadiazole and benzene rings [minimum ring centroid separation = three.7706 (14) A].The authors thank the Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq), the Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES), the ` Fundacao de Amparo a Pesquisa e Inovacao do Estado de Santa Catarina (FAPESC), the Financiadora de Estudos e ^ Projetos (FINEP) plus the Instituto Nacional de Ciencia e lise for monetary help. Tecnologia (INCT) – CataSupporting details for this paper is readily available from the IUCr electronic archives (Reference: ZS2285).Associated literatureFor the bioactivity of 1,3,4-oxadiazole Trk Receptor Gene ID derivatives, see: Bostrom et al. (2012); Rajak et al. (2009); Polshettiwar Varma (2008). For the properties of the 1,three,4-oxadiazole heterocycle, see: Bolton Kim (2007); Liu et al. (2007); Kulkarni et al. (2004). For material chemistry applications, see: Hughes Bryce (2005); Wang et al. (2011); Cristiano et al. (2006); Han (2013). For the synthesis, see: Gallardo et al. (2001). For relate.